EpoxyMount Use & Mixing Instructions
Also listed as: PRODUCT USE INSTRUCTIONS
Full searchable text · 2 pages
Refer to the original PDF for tables, figures and page layout.
Page 1 Product Guide EpoxyMount Epoxy Mounting Resin Date: 02/2021, v1.7 Refer to the SDS document for additional safety information. EpoxyMount is a clear, 2-hour, room temperature curing, cold mounting epoxy resin for potting/encapsulation of metallographic samples. It exhibits excellent adhesion, very low shrinkage, and low viscosity, allowing it to penetrate open pores and cavities to maximize edge retention and support. Instructions 1. Clean the sample using micro organic soap, isopropyl alcohol and/or an ultrasonic cleaner to improve mounting material adhesion and prevent outgassing. Dry with heat or clean air to remove all moisture prior to mounting. 2. Using a scale with 0.1 g precision, weigh and mix components in a single plastic cup. Note: Do not use wax lined or paper cups. Unless they are cooled in water, the use of disposable mounting cups is also not recommended to avoid melting the cup itself. 3. Mix thoroughly by scraping both the sides and bottom of the mixing cup for approximately 2-3 minutes until the mixture appears homogenous. 4. Pour the mixture over the sample in the mounting cup. 5. Let the mount harden/cure. Note: If pouring more than 200 g of epoxy at once, the epoxy may generate too much heat and cause smoking and fuming, as well as degradation of the sample and the mold. Reducing the amount of epoxy mixed and poured at once may help reduce heat and allow for a better cure. It is recommended to mix about 150 g at a time and to pour no more than can cover 0.5"-1" segments. Use of a conductive mold, like a steel cylinder, can also reduce heat. Eliminating Bubbles & Air Pockets Vacuum impregnation and/or a pressure chamber can be used to eliminate bubble formation by filling open pores and cavities, which can interfere with adhesion of the mounting resin to the sample and can collect debris during grinding and polishing. Debris will contaminate the polishing cloths, leaving scratches on the polished surface. After pouring the epoxy, place the cup into the vacuum chamber and vacuum for 3-5 minutes at 25-30 inHg. Release the vacuum slowly. Then, cure the mount in a pressure chamber at 25-30 psi. Technical Information Mixing Ratio (by weight) 10:3 (Resin: Hardener)* Mixed Viscosity 350-500 cP Curing Schedule (Room Temperature) (1.25" ø x 1" H mount) 2 hours* Pot Life 25 minutes at 100 g Peak Exothermic Curing Temperature 66 °C (150 °F)* Durometer Hardness 87D Shrinkage 0.00008%, Inch/Inch Izod Impact/Tensile Strength 0.94/7600 psi Glass Transition Temperature 140 °C (284 °F) Light Refractive Index 1.519 * Optimum mixing ratio; larger volume mixtures cure at higher temperatures and faster rates. GHS07 GHS05 GHS09 www.alliedhightech.com Allied High Tech Products, Inc. Call for more information: 800.675.1118 Page 2 www.alliedhightech.com Allied High Tech Products, Inc. Call for more information: 800.675.1118 2 of 2 Table 1: EpoxyMount Standard Curing Parameters Mount Size Cure Time (Hours)* Mixing Ratio Weight (g)** Resin Hardener 1"/ 25 mm 2-3 10:3.5 10.77 3.77 1.25"/ 32 mm 1.5-2 10:3 17.5 5.25 1.5"/ 38 - 40 mm 1-1.5 10:3 25.19 7.56 2"/ 50 mm 1-2 10:2.5 36.67 9.17 * Variations in room temperature and mixing ratios will influence performance and the data in the table above. The larger the mass, the higher the exothermic temperature reached during curing and the faster the epoxy will cure. Place large molds into a shallow bath of water to reduce exothermic heat. Measure both parts with the same cup. ** Per one (1) mount 45-Minute Cure Time The cure time for EpoxyMount can be shortened from 2 hours to 45 minutes by adding heat. Once a mount is ready to cure, heat it on a hot plate or in an oven at 38 °C (100 °F) for 10-15 minutes. This is not recommended for heat-sensitive specimens. Back-Filling Back-filling is a process where a sample with an inaccessible area that needs support is mounted, ground to expose the air pocket and then remounted in epoxy. Vacuum is used to pull the air from the pocket that is displaced with epoxy, providing support to the structure. When back-filling, be sure to use enough epoxy to fully cure and harden. Crystallization When stored in cool conditions, crystallization of the resin (Part A) may occur. To dissolve the crystals, loosen the cap and heat the bottle to 38 °C (100 °F) for 30 minutes. Allow it to cool to room temperature before using. Sample Removal EpoxyMount is non-soluble in water when cured. If a sample needs to be removed from epoxy that is cured or not fully cured, it can be dissolved using Allied’s Epoxy Dissolver (#145-50210). The time required to dissolve the epoxy can be reduced if the excess is ground or cut prior.